{"id":386,"date":"2020-11-09T14:41:55","date_gmt":"2020-11-09T05:41:55","guid":{"rendered":"https:\/\/integ.synfoster.hokudai.ac.jp\/lab\/shinozaki\/?page_id=386"},"modified":"2022-01-17T12:27:40","modified_gmt":"2022-01-17T03:27:40","slug":"facilities","status":"publish","type":"page","link":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/en\/facilities","title":{"rendered":"Facilities"},"content":{"rendered":"

The laboratory and facilities are belong to Earth Materials Science Group\u3000(4G)<\/a>.<\/p>\n

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High-Pressure and High-Temperature Apparatuses<\/h3>\n

Diamond Anvil Cells(DAC)<\/h4>\n

The sample is compressed between two opposed diamond anvils which can generate quite high pressure > 50 GPa. There are many kinds of cell type in our lab.; Cramp type, Symmetric type, Mao-Bell (lever) type.<\/p>\n

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Resistance-Heating Diamond Anvil Cells<\/span><\/h4>\n

The sample can be heated with a few hundred of degrees Celsius under high pressures by combining with a resistance-heating coil adjusted on the diamond anvil cell.<\/p>\n

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Other Experimental Equipment for DAC<\/h4>\n
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A spot welder and precise drilling machines for drilling the sample hole in the gasket.<\/p>\n<\/div>\n<\/div>\n

Piston Cylinder Type Apparatus with a Resistance Heating<\/span><\/h4>\n
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A piston cylinder with a hand press. We use it for synthesizing large volume samples under pressure conditions up to 1.5 GPa, 350 \u2103.<\/p>\n<\/div>\n<\/div>\n

Characterization facilities<\/h3>\n

Micro-Raman spectrometer<\/h4>\n
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The diode laser (532 nm) is used as an excitation light source. Use for obtain Raman spectra of materials at ambient condition and at high-pressure and high-temperature conditions combined with DAC. Also, ruby fluorescence spectra are measured for pressure determination.<\/p>\n<\/div>\n<\/div>\n

Ultraviolet Visible Absorption Spectroscopy (UV-vis)<\/span><\/h4>\n
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Use for the measurements of absorption spectroscopy of solutions and solids from ultraviolet to visible spectral regions.<\/p>\n<\/div>\n<\/div>\n

GC\/MS<\/h4>\n
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Use for the measurement on mass spectrometry of organic materials.<\/p>\n<\/div>\n<\/div>\n

FT-IR<\/h4>\n
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Use for the measurements of infrared spectra. Micro IR spectra on high-pressure conditions are measured combined with the cramp type DAC.<\/p>\n<\/div>\n<\/div>\n

\u203bWe also use Synchrotron X-ray diffraction measurement system on KEK-PF BL18-C, neutron diffraction measurement system on J-PARC MLF PLANET beam-line.<\/p>\n

Pictures of the Laboratory<\/h3>\n
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The laboratory and facilities are belong to Earth Materials Science Group\u3000(4G). High-Pressure and High-Tempera […]<\/p>\n","protected":false},"author":2,"featured_media":0,"parent":28,"menu_order":2013,"comment_status":"closed","ping_status":"closed","template":"","meta":[],"_links":{"self":[{"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/pages\/386"}],"collection":[{"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/users\/2"}],"replies":[{"embeddable":true,"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/comments?post=386"}],"version-history":[{"count":3,"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/pages\/386\/revisions"}],"predecessor-version":[{"id":735,"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/pages\/386\/revisions\/735"}],"up":[{"embeddable":true,"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/pages\/28"}],"wp:attachment":[{"href":"https:\/\/c-mng.cwh.hokudai.ac.jp\/mineral-shinozaki.sci\/Root\/wp-json\/wp\/v2\/media?parent=386"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}